Validation and determination of the contents of acetaldehyde and formaldehyde in foods
- 주제(키워드) Acetaldehyde (AA) , Food products , Formaldehyde (FA) , GC-MS , SPME , Validation
- 등재 KCI등재, SCOPUS
- 발행기관 Korean Society of Toxicology
- 발행년도 2015
- 총서유형 Journal
- URI http://www.dcollection.net/handler/ewha/000000120451
- 본문언어 영어
- Published As http://dx.doi.org/10.5487/TR.2015.31.3.273
초록/요약
The aim of this study was to develop an efficient quantitative method for the determination of acetaldehyde (AA) and formaldehyde (FA) contents in solid and liquid food matrices. The determination of those compounds was validated and performed using gas chromatography-mass spectrometry combined by solid phase micro-extraction after derivatization with O-(2,3,4,5,6-pentafluoro-benzyl)-hydroxylamine hydrochloride. Validation was carried out in terms of limit of detection, limit of quantitation, linearity, precision, and recovery. Then their contents were analyzed in various food samples including 15 fruits, 22 milk products, 31 alcohol-free beverages, and 13 alcoholic beverages. The highest contents of AA and FA were determined in a white wine (40,607.02 ng/g) and an instant coffee (1,522.46 ng/g), respectively.
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